Paul Industries plans and executes shutdown, purging and turnaround work at North Dakota crush and solvent extraction plants. Cleaning a solvent plant has almost nothing in common with cleaning a food plant. Nobody is worried about residue. The entire exercise is about getting a flammable solvent out of a system completely enough that people can open it and work inside it, and then getting it back into service without introducing an atmosphere that will burn.

Request a quote or call 201-450-8280

The objective A system safe to open, enter and work in
The sequence Drain, steam or purge, inert, gas test, then work
The hazard on restart Passing back through the flammable range in the other direction
The paperwork Isolation, confined space and hot work permits, all live at once
Industrial power 7.25 cents/kWh, 0.89x the US average of 8.13 (EIA, 2024)
Reviewed September 2026, against current state code and EIA 2024 energy data

Getting the solvent out, in order

North Dakota’s crush plants run long campaigns and shut down rarely, which concentrates a great deal of work into a short window and makes the preparation sequence worth getting right rather than improvising.

Drain, and know where liquid hides. Low points, dead legs, instrument tappings, the bottom of vessels, pump casings, filter housings and anything sloping the wrong way. Liquid hexane left in a pocket will evaporate slowly for as long as the system is open and will keep regenerating an atmosphere that gas testing had already cleared. A system that can be genuinely drained is a system designed for it, which is a point that belongs in the original design rather than in the turnaround plan.

Steam or purge to remove what draining left. Steaming out is effective because it both displaces vapor and warms surfaces so adsorbed solvent releases, and it leaves the system hot and wet, which has consequences for corrosion covered on our North Dakota corrosion page. Nitrogen purging is the alternative where steam is unsuitable, and it introduces an asphyxiation hazard in exchange for removing a fire one.

Inert before you are in the flammable range, not after. This is the critical technical point of the whole exercise. A vessel full of hexane vapor is above the upper flammable limit and will not burn. A vessel full of air will not burn either. Going directly from one to the other passes through the flammable range, and doing so with any ignition source present is how these events happen. Displacing with nitrogen first means the transition happens with insufficient oxygen to support combustion at any point.

Gas test, then keep testing. A single clear reading at the start of a shift is not a license for the day. Conditions change as residual liquid evaporates, as temperature rises, and as work disturbs deposits. Continuous monitoring during work, not a test before it.

Isolate physically. A closed valve is an operational isolation and it will eventually be opened by someone who does not know. Blinds, spades or spool removal are what make a line genuinely dead, and the isolation register has to be as carefully managed as the work itself.

Three permits, one job

A typical turnaround activity inside a crush plant sits under several permit regimes simultaneously, and the interaction is where mistakes occur.

Overlapping requirements on a single task
RegimeAsksInteraction risk
Energy isolationIs it positively isolated and verified?Re-energized for testing mid-job
Confined space entryAtmosphere, attendant, rescue planNitrogen inerting creates the hazard
Hot workGas testing, fire watch, no flammablesAdjacent system still in service
Line breakingDrained, depressurized, isolatedResidual liquid in a low point

The confined space row contains the contradiction worth naming. Inerting a vessel with nitrogen makes it safe from fire and lethal to enter, and people have died entering vessels that were correctly inerted precisely because the inerting worked. A vessel that has been nitrogen purged must be air-purged and verified for oxygen before anyone goes in, and the sequence of those two operations, inert for the work outside, then air purge for the work inside, has to be planned rather than assumed.

The hot work row contains the other one. Welding on a line that has been cleared, in a building where an adjacent system is still running, means the gas test result describes the line rather than the room. Both need testing, and the room test needs repeating.

Restart, which is the other half of the risk

Attention concentrates on shutdown and the restart is frequently treated as simply reversing it. It is not symmetrical, and the flammable range has to be crossed again in the opposite direction.

The same principle applies: purge the air out with nitrogen before introducing solvent, so the system never contains a mixture of hexane and sufficient oxygen at the same time. A restart that admits solvent into an air-filled system passes through the flammable range with a plant full of hot surfaces and running equipment.

Two further restart considerations recur.

Verify the isolations were removed. A blind left in place is discovered as a pressure excursion or a pump running dead-headed, and the register that recorded its installation is the only reliable way to be sure it came out.

Leak test before full operation. Every joint broken during the turnaround is a potential leak, and finding them at low pressure with an inert medium is considerably better than finding them with hexane at temperature.

Turnaround support electricity at North Dakota’s 7.25 cents/kWh
Continuous loadNorth Dakota per yearAt the 8.13 cent US average
25 kW$15,878$17,805
50 kW$31,755$35,609
100 kW$63,510$71,219

At 7.25 cents per kilowatt-hour, below the national average of 8.13 (EIA, 2024), the utilities consumed during a turnaround are a minor line. What governs the cost is duration, because a crush plant not crushing is not earning, and the single largest determinant of duration is how well the preparation was planned before the plant came down.

We plan and execute turnaround piping work on this basis: isolation and blinding schedules prepared in advance, purge and inerting sequences agreed with the plant, materials and fabrication completed before the shutdown starts, and the restart sequence written down rather than worked out on the day. We would rather spend a week on the plan than a day extra on the outage.

Frequently asked questions

Do you carry out turnaround work at North Dakota crush plants?

Yes, across Casselton, Spiritwood, Fargo, Grand Forks, Jamestown and statewide: isolation and blinding schedules, purge and inerting sequences, piping replacement and modification, leak testing and restart support, planned and materialized before the shutdown begins.

How is cleaning a solvent plant different?

Residue is not the concern. The exercise is getting flammable solvent out completely enough that people can open and enter the system, then returning it to service without creating an atmosphere that will burn. It is a hazard control operation rather than a hygiene one.

Why does draining matter so much?

Because liquid left in a low point, dead leg, instrument tapping or pump casing evaporates slowly for as long as the system is open, regenerating an atmosphere that gas testing had already cleared. A genuinely drainable system is one that was designed to be.

Why inert before opening to air?

Because going directly from a vapour-filled system to an air-filled one passes through the flammable range. Displacing with nitrogen first means the transition happens with insufficient oxygen to support combustion at any point. It is the critical technical step of the whole sequence.

Is one gas test enough?

No. Conditions change as residual liquid evaporates, as temperature rises and as work disturbs deposits, so a clear reading at the start of a shift is not a license for the day. Continuous monitoring during work is the appropriate standard.

What is the danger with nitrogen inerting?

It makes a vessel safe from fire and lethal to enter. People have died entering vessels precisely because the inerting worked. A nitrogen-purged vessel must be air-purged and verified for oxygen before entry, and the order of those operations has to be planned rather than assumed.

Why are closed valves not sufficient isolation?

Because a closed valve is an operational isolation that someone will eventually open. Blinds, spades or spool removal make a line genuinely dead, and the isolation register needs managing as carefully as the work, because a blind left in is discovered as a pressure excursion.

Is restart just the reverse of shutdown?

No, and treating it that way is where risk concentrates. The flammable range has to be crossed again in the other direction, so the system must be nitrogen purged before solvent is admitted rather than after, with hot surfaces and running equipment present.

Should we leak test before full operation?

Yes. Every joint broken during the turnaround is a potential leak, and finding them at low pressure with an inert medium is considerably better than finding them with hexane at operating temperature in a classified area.

How do I get a quote for a North Dakota turnaround?

Use the form on this page or call 201-450-8280. Useful inputs are the planned window and scope, area classification drawings, existing isolation points and whether a blinding schedule exists, and what work could be completed before the plant comes down.

What is the correct order for removing hexane from a solvent plant?

Drain liquid solvent from every vessel and low point, steam or purge to strip absorbed solvent from meal and surfaces, vent to a safe location, then inert or ventilate to bring the atmosphere below the lower flammable limit, and test before opening. Skipping the stripping step leaves solvent that reappears as vapour once the system warms.

Why does meal hold so much solvent?

Extracted meal is porous and retains hexane in its structure, and the desolventizer-toaster is designed to remove most of it during normal operation. At shutdown, meal left in equipment continues to release vapour for a long time, which is why the meal side has to be emptied and stripped rather than just stopped.

What instruments confirm a solvent vessel is safe to enter?

A calibrated multi-gas meter reading oxygen, lower explosive limit and any toxic gases the process presents, used at multiple points in the vessel including low points where hexane vapour collects, with the readings recorded on the entry permit. A single reading at the manway is not a test of the vessel.

What are the three permits involved in a turnaround?

Typically a hot work permit for any ignition source, a confined space entry permit for vessel entry, and a line-break or isolation permit for opening equipment that contained solvent. Each has its own conditions, and the sequence has to satisfy all three at the moment work starts.

What does positive isolation of solvent equipment involve?

Physical disconnection or blinding of every line into the equipment, with the blinds listed and tagged, and with valves closed and locked only as a supplementary measure. A blind list is part of the turnaround plan, and the equipment is not opened until every line on the list is blinded.

What has to be true before solvent is reintroduced after a turnaround?

Every blind removed and confirmed against the list, the equipment leak tested, inert purge completed to remove air, instrumentation and interlocks proven, and the area classification restored with hot work stopped. The reintroduction is a permit step, not an operational one.

How is the inert gas supply sized for a plant-wide purge?

From the volume of the equipment being inerted, the number of volume changes needed to reach the target oxygen level, and the rate at which the purge has to complete within the turnaround window. Undersized supply is the usual reason a purge runs long, and a purge that runs long delays every task behind it.

What about the crude oil and refining side during a turnaround?

Refining equipment carries oil, caustic and bleaching earth rather than solvent, and its cleaning is a fouling and corrosion question rather than a flammability one. The two sides are planned as separate work packages with separate hazards.

How long does a proper turnaround take?

It depends on the scope, but the fixed elements are the solvent removal and atmosphere testing at the start and the leak testing and inerting at the end. Compressing those is where accidents come from; compressing the maintenance in between is where planning pays.

Where does the solvent go during shutdown?

To storage, recovered by the plant's own condensing and recovery system as far as possible, with the remainder vented through a safe route. Solvent losses at turnaround are both a cost and an environmental reporting item, and the recovery plan reduces both.

How is dust handled during turnaround on the preparation side?

Grain dust accumulations in the prep and meal areas are removed before hot work anywhere nearby, because a turnaround introduces ignition sources into a building full of fuel. Dust cleaning is a pre-turnaround task, not a maintenance afterthought.

What instrumentation should be verified at restart?

Solvent vapour detectors, oxygen monitors, temperature and pressure instruments on the extractor and desolventizer, and interlocks that stop the process on high vapour or loss of ventilation. Instruments that were disconnected for maintenance are a common restart finding.

Can a crush plant clean its extractor without a full shutdown?

Not safely. The extractor contains solvent and meal, and any cleaning that requires opening it needs the full removal and isolation sequence. Design changes that reduce fouling in the extractor are the way to reduce the frequency of the full shutdown.

How does cold weather affect turnaround work in North Dakota?

Water used for washing freezes, steam lines and condensate systems are at risk, and workers in cold conditions make more errors. Winter turnarounds need heated work areas, protected water systems and more time for each step.

Do you plan and execute the turnaround, or only advise?

We plan the sequence, prepare the isolation and permit documentation with the plant, and execute the mechanical work, with the plant's own safety system governing permits and entry. The division of responsibility is agreed in writing before the shutdown starts.

Planning a North Dakota crush plant turnaround?

Send the scope and the area classification drawings early. Everything that can be fabricated before the plant comes down is a day off the outage. Call 201-450-8280 or use the form below.

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